Compose your shot first, in focus, and then switch to manual. Otherwise the camera will try (and fail) to lock onto something through an almost black filter.
Then screw the filter on and use bulb (doing a ten stop calculation, or guessing the exposure time).
Works best with flowing water and/or moving clouds
Its a bit fiddly having to unscrew the filter to compose each time but its worth it. Enjoy!
- that nicely sums it up Simon^ I find this too Matt. I take a reading without the filter then add around 12 stops with the filter on.
Any tips? ... Buy a camping stove, bring a kettle and a few tea bags.
Set up the shot.
Attached new filter
Release shutter
Put on the kettle
Have a nice cup of tea
Close shutter.
Check histogram
Why do you add 12 stops, if you don't mind me asking?!
Do you think that's a case with your filter only? I ask, as mine come out just about perfectly exposed when I adjust for the 10 stops exactly; and I do an additional adjustment of 1/2 a stop as I like my shots slightly over exposed. But 2 stops is a big deviation :shrug:?!

I suspect that the viewfilnder cover on my camera isn't 100% lightproof so this might account for any underexposure, but I'm purely guessing